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SRPS EN 12766-2:2011

Petroleum products and used oils - Determination of PCBs and related products - Part 2: Calculation of polychlorinated biphenyl (PCB) content

Mar 31, 2011

General information

90.93     Apr 10, 2012

90.00    Mar 23, 2017

ISS

B028-1

European Norm

75.080     75.100  

English  

po planu za 2010. godinu

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Scope

This standard specifies two calculation procedures ("method A" and "method B") for PCB content. The basis for this quantification is taken from the chromatographic results of EN 12766-1:2000 in which all necessary experimental procedures are described for the specific analysis of unused, used and treated (e.g. dechlorinated) petroleum products including synthetic lubricating oils and mixtures of vegetable oils. The method is also applicable to petroleum products and synthetic lubricating oils suitably recovered from other materials, e.g. from waste materials. Both methods have different strengths and weaknesses which are described in the next paragraphs and which must be considered before use in a specific application. Proper application of either method A or method B needs to be carefully considered before use in a specific application.

Using method A, special care needs to be exercised to avoid interferences from non PCB substances which may occur in the chromatogram. Therefore, method A can be used predominantly for the analysis of used and unused insulating oils. It is recommended not to use calculation method A without special precautions for other than above-mentioned products. Calculation method A can produce two alternative sets of results, ("All Probables" and "All Possibles"). Therefore, care needs to be taken in order to interpret these results in the correct manner.

Method B uses as intermediate result the sum of six congeners, which belong to the most abundant in almost all technical PCB materials, thereby minimizing potential interferences from other (coeluting) non PCB substances. To obtain the PCB content, the intermediate sum from six congeners needs to be multiplied by a multiplication factor. Calculation Method B can be used predominantly for the analysis of liquids from used and waste materials of unknown origin and for samples with low PCB contents.

Life cycle

NOW

PUBLISHED
SRPS EN 12766-2:2011
90.93 Standard confirmed
Apr 10, 2012

Related project

Adopted from EN 12766-2:2001

National regulations and standards

"Сл. гласник РС" бр. 65/2011 и 17/2017 "Сл. гласник РС" бр. 65/2011 и 17/2017
PRAVILNIK o izmenama Pravilnika o listi POPs materija, načinu i postupku za upravljanje POPs otpadom i graničnim vrednostima koncentracija POPs materija koje se odnose na odlaganje otpada koji sadrži ili je kontaminiran POPs materijama

МИНИСТАРСТВО ПОЉОПРИВРЕДЕ И ЗАШТИТЕ ЖИВОТНЕ СРЕДИНЕ