SRPS EN 14185-2:2008

Non fatty foods - Determination of N-methylcarbamate residues - Part 2: HPLC method with clean-up on a diatomaceous earth column

Scope

This draft European Standard specifies a high performance liquid chromatographic (HPLC) method for the determination of residues of N-methylcarbamate pesticides in fruits and vegetables and is based on the method of Krause [1].
The method has been validated by collaborative study for aldicarb, carbofuran, furathiocarb, methomyl, oxamyl, propoxur and thiodicarb parent compounds and for the metabolites aldicarb sulfoxide, aldicarb sulfone (aldoxycarb) and 3-hydroxy-carbofuran in tomatoes and oranges at levels between 0,04 mg/kg and 0,25 mg/kg.
No collaborative data are available for the performance of the method in the determination of other significant compounds although it is known that the method is unsatisfactory for benfuracarb.