Objavljen
The determination is carried out in the following way: Decomposition of the soap by sulfuric acid and extraction of the fatty acida with light petroleum. Oxidation of the free glycerol remaining in the aqueous phase by periodic acid to formic acid and formaldehyde. On reaction with chromotropic acid, the aldehyde formed gives an absorbing compound whose absorbance is propotional to the free glycerol content. Spectrometric measurement of the absorbance at a wavelength about 571 mm.
POVUČEN
ISO 2272:1972
OBJAVLJEN
ISO 2272:1989
90.60
Završetak postupka preispitivanja standarda
3. 9. 2026.
Površinski aktivne materije - Sapuni - Određivanje niskih sadržaja slobodnog glicerina molekularnom apsorpcionom spektrometrijom (identičan sa ISO 2272:1989)
90.60 Završetak postupka preispitivanja standarda