Objavljen
This document specifies a method for the determination of certain cyclic volatile methylsiloxanes (cVMS) in environmental water samples with low density polyethylene (LDPE) as a preservative and subsequent liquid-liquid extraction with hexane containing 13C-labeled cVMS as internal standards. The extract is then analysed by gas chromatography-mass spectrometry (GC-MS).
NOTE Using the 13C-labeled, chemically identical substances as internal standards with the same properties as the corresponding analytes, minimizes possible substance-specific discrimination in calibrations. Since these substances are least soluble in water, they are introduced via the extraction solvent hexane into the system.
OBJAVLJEN
ISO 20596-2:2021
90.60
Završetak postupka preispitivanja standarda
5. 6. 2026.
Kvalitet vode – Određivanje cikličnih isparljivih metilsiloksanata u vodi – Deo 2: Metoda za tečno-tečnu ekstrakciju na gasnoj hromatografiji sa masenom spektrometrijom (GC-MS)
60.60 Standard objavljen